Authors | Hamid Beyzaei |
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Journal | Molecular Catalysis |
Page number | 1-10 |
Serial number | 45 |
Volume number | 526 |
Paper Type | Full Paper |
Published At | 2022 |
Journal Type | Typographic |
Journal Country | Netherlands |
Journal Index | ISI،JCR،Scopus |
Abstract
A novel and green protocol was developed for the synthesis of amides via the reaction of benzyl alcohols with amines in the presence of Ni-MOF named UoB-8 as catalyst. The morphological, structural, and physicochemical characteristics of the Ni-MOF were investigated by FT-IR, XRD, FESEM, EDX, TEM, BET, CHN and ICP analyses. The products were obtained in good to excellent yields, with short reaction times, under ultrasound irradiation (40 ºC) in ethanol as solvent. In addition, low-cost catalyst was recovered and reused at least 5 times without detecting a noticeable reduction in efficiency.
tags: Ni-MOF, Cascade Oxidative, amidation Alcohol Ultrasound,-irradiation